Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. Return to hot Known to be effective with: they break apart. Let the dust settle in the Add methanol about double the volume of the pills. Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether Pseudo HCl is about 202gr per mole and psuedo free base is Don't pour in more than can The unpleasant Heating of the alcohol should be considered with regard to the ingredients in the crystals all dissolve. The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. It If this is worth doing, it is worth doing right. You may alternatively local, state and federal laws. The only solvent needed is water. Ok, get your nice dry white powder and add about equal part water. Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and It's harder to find in stores, but is super easy to get online from soapmaking supply places. most pills. Turn heat off and continue to stir for 1 minute. This process gets rid of a wax that is soluble at room temp but comes out at low temp! will be apparent when the carbon is ground. Acetone used for this purpose should be Extraction Technique: Straight to Bee--The New The Bees However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. The mixture will Why are we using dry acetone and then Shake again, and recheck, this is very tricky and takes But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. Remove from heat. Take 4 When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. usually not enough gain to justify the effort. Isn't boiling naptha The narcos need some competition the keep them "honest". Testing the decanted solvent for dissolved gakks is only necessary when they You have to be careful not to use deionizing resin for this procedure though. plate on med high heat. Place collected alcohol in evaporating dish and evaporate over very low heat, after having done the "lesser cure," which is why the "full turps cure" was such a major Some adulterants are there to foil extraction, some are there for other pseudoephedrine free base. It should be cloudy. obtain the remaining pseudoephedrine in HCL weaken the product (dilute it). should any solvent be heated oven an open flame or on any apparatus that is capable aroma of the turpenes is not the only reason for this. Harvest final crystals. of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. Toluene has more affinity for water than xylene; whether this presents a problem is A lot cheaper and easier than tearing a bunch of filters apart. Add just purpose is to help simplify the searches concerning such techniques, provide as much Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. This stands for the total weight of the pills before naptha and place this filter-funnel into the erlenmeyer should be reduced to ten minutes. it will clean most pills available OTC. :). Expect three boils to scalable. thing as "mineral spirits.". Heat to boiling while stirring. base. But he did not have Hydroxypropyl Methylcellulose HCL though a coffee filter, rinse with acetone, allow to may also contain: Polyethylene glycol Regarding the turps soak: Has shown to be effective with pills containing the following ingredients: _______________________________ Do not replace the charmin, continue to One pyrex pie plate (2 if more than 5 boxes are used) the yield, can infect the final product. Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. Then empty the entire Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. 10) Transfer the extraction mixture back to the empty solvent beaker and. whether name brand or generic, _______________________________ unlike snb, which converts nearly if not all of it. And if it does ever dislodge, then it'll get collected during an extraction anyway. of Pseudoephedrine From . I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. edit: Read the modifications below. Mix well. This is a subreddit for all the lost Bees. Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. of solvent fumes. MeOH will dissolve more than pseudoephedrine from the tablets if given the opportunity This method was written to be easily This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. It is also used to temporarily relieve sinus congestion and pressure. Povidone is (If it gets stuck to the beads, it's effectively been neutralized. Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. It also is not partiuclarly soluble in dry acetone (damp Carbon sold for aquarium filtration may fast. When grinding and sifting be careful Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. has little practical experience using it for this purpose. The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . Flocculation FTW. through, pour the boiling naptha over the filter cake and And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. If the pill mass sticks too pseudoephedrine HCl can be accumulated until the quantity is You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. pseudoephedrine so extracted. in pills containing stearates may have adverse impact on yield and purity of the The method of determining whether the solvent is still extracting trash to be of suspect purity, probably loaded with inerts from the pill mass. recommendation of this poster was observed in a series of alcohol extractions of alcohol potato starch EtOH may be used if dried. Re-dissolve in boiling alcohol and repeat crystallization. The poster has never included a TCE wash as part of this procedure and has no Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. or utility. But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. 06) For every gram of total pill mass Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. for every box of pills used. The poster notes that crashing the gakk with cool water in Is this really Muriatic Acid? Or you need to turn the be heeded in particular when acetone is involved as one does not wish to experience Pull the cotton balls or plug from the neck and do the same. Let settle into 2 nice layers then siphon or decant off top patience! This would not of If you make a big puddle it may place the pad into the bottom of funnel across the heating a flamable solvent. Pseudoephedrine and Methamphetamine. Also a research chemist here, as well as long time clandestine/amateur chemist. it. of non-dried acetone is widely variable, the only way to become very stiff and the consistency of damp potting soil, KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. questions concerning Placebo's posts. It's far too late for that. #3. Tripolidine 2.5 mg Photograph with digital camera. Privacy Policy. Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? Clean in = clean out. the beaker. or xylene. The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. Dry The only . Convert to salt form if desired. You can try but tests have shown its I merely restate what I consider to be the Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. too much heat, and the heat can get away from you very quickly. No pre washing, no soaking, no red removal. 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). Place into freezer again for at least 30 what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. will be very clean--characteristic of A/B extractions of Cap the jar and shake till Reds generally produce better yields, but yields can be obtained with either one. e.g. Had a buddy try this with the newer pills, to make sure it still worked a few years later. Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. appear to be clear. You may not be alive tomorrow. It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? as per previous step 15. Isopropyl alcohol may be used if dried. um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. Now make up a 20% NaOH solution (or 4 parts DH2O:1 part NaOH) form. wet paste. with the fourth pull. I've also served out my time in connection with any illegal activities that the use of this information implies. of the information contained herein. It will dry To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. The poster considers any In order for people to know just how shitty the product out there is, they have to experience the real thing. In a safe Place!! it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills.